BS ISO 7981-1-2005 水质.测定多核芳香烃类(PAH).液液萃取后用带荧光检测的高效薄层色谱法测定六PAH

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【英文标准名称】:Waterquality-Determinationofpolycyclicaromatichydrocarbons(PAH)-DeterminationofsixPAHbyhighperformancethinlayerchromatographywithfluorescencedetectionafterliquid-liquidextraction
【原文标准名称】:水质.测定多核芳香烃类(PAH).液液萃取后用带荧光检测的高效薄层色谱法测定六PAH
【标准号】:BSISO7981-1-2005
【标准状态】:现行
【国别】:英国
【发布日期】:2005-08-01
【实施或试行日期】:2005-08-01
【发布单位】:英国标准学会(BSI)
【起草单位】:BSI
【标准类型】:()
【标准水平】:()
【中文主题词】:质量;芳烃;萃取;含量测定;多核芳香烃类;水质;薄层色谱法;可溶的;水;试验;饮用水;色谱法;烃类
【英文主题词】:Aromatichydrocarbons;Chromatography;Determinationofcontent;Extraction;Hydrocarbons;Polynucleararomatichydrocarbons;Potablewater;Quality;Soluble;Testing;Thin-layerchromatography;Water;Waterquality
【摘要】:ThispartofISO7981specifiesthedeterminationofsixselectedPAHindrinkingwaterbyhigh-performancethin-layerchromatographywithfluorescencedetectionafterliquid-liquidextraction.ThesixPAHare:fluoranthene,benzo[b]fluoranthene,benzo[a]pyrene,benzo[k]fluoranthene,indeno[1,2,3-cd]pyrene,andbenzo[ghi]perylene(seeTable1).Ascreeningmethod(methodA)isdescribedtoexcludethosesamplescontaininglessthan20%ofthelimitvaluesgiveninReferences[1],[2],[3]and[4].Aquantitativemethod(methodB)isalsodescribed,withaworkingrangeof40ng/lto240ng/l(sumof6PAH).Higherconcentrationscanbedeterminedbyusingasmalleraliquotofthesample.Withsomemodifications,thismethodisalsoapplicablefortheanalysisofgroundwatersandmoderatelypollutedsurfacewaters.
【中国标准分类号】:Z16
【国际标准分类号】:13_060_50
【页数】:32P.;A4
【正文语种】:英语

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上一篇: BS ISO 7981-2-2005 水质.测定多核芳香烃类(PAH).液液萃取后用带荧光检测的高效液相色谱法测定六PAH
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【英文标准名称】:StandardPracticeforSeparationandConcentrationofIgnitableLiquidResiduesfromFireDebrisSamplesbySolventExtraction
【原文标准名称】:用溶剂萃取法分离和浓缩从火烧瓦砾样品中获取的可燃液体残渣的标准实施规程
【标准号】:ASTME1386-2000(2005)
【标准状态】:现行
【国别】:
【发布日期】:2000
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:E30.01
【标准类型】:(Practice)
【标准水平】:()
【中文主题词】:溶剂;分析方法
【英文主题词】:firedebris;samples;solventextraction
【摘要】:Thispracticeisusefulforpreparingextractsfromfiredebrisforlateranalysisbygaschromatography,GC/MS,orGC/IR.Thisisaverysensitiveseparationprocedure,capableofisolatingquantitiessmallerthan1x03BC;Lofignitableliquidresiduefromasample.Thispracticeisparticularlyusefulwhenthepotentialforfractionationduringseparationmustbereduced,aswhenattemptingtodistinguishbetweenvariousgradesoffueloil.Thispracticeisparticularlyusefulfortheextractionofnonporoussurfacessuchasglass,ortheinteriorofburnedcontainers.Itisalsoparticularlywellsuitedtotheextractionofmaterialsfromverysmallsamples.Thispracticecanbehamperedbycoincidentextractionofinterferingcompoundspresentinthefiredebrissamples.ThispracticemaynotbeusefulfortheextractionofsomeClass0andClass1ignitableliquids,whichmayevaporateduringtheconcentrationstep.Thisisadestructivetechnique.Wheneverpossible,thistechniqueshouldonlybeusedwhenarepresentativeportionofthesamplecanbereservedforreanalysis.Thoseportionsofthesamplesubjectedtothisproceduremaynotbesuitableforresampling.ConsiderusingpassiveheadspaceconcentrationasdescribedinPracticeE1412.1.1Thispracticecoverstheprocedureforremovingsmallquantitiesofflammableorcombustibleliquidresiduefromsamplesoffiredebrisusingsolventtoextracttheresidue.1.2Thispracticeissuitableforsuccessfullyextractingflammableorcombustibleliquidresiduesovertheentirerangeofconcentrations.1.3AlternateseparationandconcentrationproceduresarelistedinTestMethodE1387.1.4Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.Foraspecifichazardstatement,seeNote1.
【中国标准分类号】:A43
【国际标准分类号】:71_040_40
【页数】:2P.;A4
【正文语种】: